150gA 60H 2 色谱柱:石英毛细管柱,DB-1701,30m×0.53mm(内径)×1.0μm(膜厚),或相当者;b)载气:氮气(纯度大于99.999%);恒压模式:89.635kPa(13psi);尾吹气流速:30mL/min;氢气流速:75mL/min,空气流速:90mL/min;c)柱温:初始温度120C保持1min,以10C/min升至230C,以20C/min升至270C保持12min;d)进样口温度:250C;e)检测器温度:250C;f)进样方式:脉冲不分流进样,脉冲压力172.375kPa(25psi),脉冲时间0.75min;g)进样量:4L;h)开阀时间:0.75min