盐酸美金刚片中N-(二甲基金刚烷)甘氨酸检测方案(液相色谱柱)
仪器: Dionex UltiMate 3000超高效液相色谱仪
色谱柱:Thermo Scientific Hypersil Gold aQ (100×2.1 mm,1.9 μm)
流动相:A为水相:0.1%甲酸水,B为有机相:乙腈
仪器:Thermo Q Exactive Focus四极杆-静电场轨道阱高分辨串联质谱
离子源参数:HESI Spray voltage: +3.5 KV; Sheath Gas Pressure: 40 arb; Aux Gas Pressure: 10 arb; Capillary Temp: 300℃; Heater Temp: 350℃