CC-505 搭配2L的Radleys反应釜中温度反应：降温，升温，可实现的最低温度检测方案(水浴、油浴)

Case Study CS 1228|205Technical details and dimensions are subject to change. No liability is accepted for errors or ommisions.www.huber-online.com React dy CC@@_505 CC-505 cycling a 2 litre Radleys jacketedreactor Requirement HH This case study demonstrates the ability of theCC-505 refrigeration bath circulator to cycle theprocess temperature in a range from +20℃to -50℃， the closeness of the temperaturecontrol and the minimum process temperatureachievable in the process mass. Method Reactor The 2 litre Radleys reactor was connected to theCC-505 using two M24x1.5 1-meter flexiblehoses. The thermofluid used in the system wasM40.165.10."Process" control was carried outvia a Pt100 sensor located in the process mass.Stirrer speed was set to 200 rpm. Setup details Temperature range： -50C...+200°C Cooling power： 1.2 kW @ +100°C 1.2kW@+20°C 1.0 kW @ 0°C 0.6 kW @ -20°C 0.15 kW @-40°C Heating power： 1.5kW Hoses： M24x1.5；2*1m HTF： M40.165.10 Reactor： Radleys 2 litre iacketed reactor Reactor content： 1.5 litre M40.165.10 Stirrer speed： 200 rpm Control： process Performance： Cooling down and heating up in a range from +20℃ to-20℃.The CC-505 needs approximately 45 minutes to cool down the reactorfrom +20℃ to -20C and 35 minutes to heat it up from -20°℃ to +20℃. Once stable at +20℃ under"Process” control， a set-point of -50C isentered. The CC-505 cools the reactor down to the minimum achievableprocess temperature of -34°C. CC®-505CC®-505 cycling a 2 litre Radleys jacketedreactorRequirementThis case study demonstrates the ability of theCC-505 refrigeration bath circulator to cycle theprocess temperature in a range from +20°Cto -50°C, the closeness of the temperaturecontrol and the minimum process temperatureachievable in the process mass.MethodThe 2 litre Radleys reactor was connected to theCC-505 using two M24x1.5 1-meter flexiblehoses. The thermofluid used in the system wasM40.165.10. “Process” control was carried outvia a Pt100 sensor located in the process mass.Stirrer speed was set to 200 rpm.Setup detailsTemperature range: -50°C...+200°CCooling power: 1.2 kW @ +100°C1.2 kW @ +20°C1.0 kW @ 0°C0.6 kW @ -20°C0.15 kW @ -40°CHeating power: 1.5 kWHoses: M24x1.5; 2* 1 mHTF: M40.165.10Reactor: Radleys 2 litrejacketed reactorReactor content: 1.5 litre M40.165.10Stirrer speed: 200 rpmControl: processresultsPerformance:Cooling down and heating up in a range from +20°C to -20°C.The CC-505 needs approximately 45 minutes to cool down the reactorfrom +20°C to -20°C and 35 minutes to heat it up from -20°C to +20°C.Lowest achievable temperature (Tmin):Once stable at +20°C under “Process“ control, a set-point of -50°C isentered. The CC-505 cools the reactor down to the minimum achievableprocess temperature of -34°C.