全自动多头熔样机操作规程

FORJ“火蝾”熔样机——源自Claisse专业熔融技术高精度元素分析强有力的保证FORJ&trade 熔样机拥有高水平的稳健性，旨在提供出色的生产力和可靠的结果，它是改变熔融法样品制备的变革者。不管您是采用 X 射线荧光法 (XRF)、电感耦合等离子体法 (ICP) 还是原子吸收法 (AA) 进行分析，FORJ 都是您的分析过程中的一个关键环节。机器稳健可靠高处理量可重复的结果机器易于集成、安装和使用机器维护需求极低，即使在恶劣条件下也不例外每家实验室都希望尽可能地减少停机时间和零件更换成本。因此，FORJ火蝾经过专门设计以减少热应力和降低污染风险，进而有效地减少维护需求，从而确保更高的效率和生产率。准确的分析结果可重复的结果是任何一个分析过程的关键目标。为此，高质量的样品制备是关键。FORJ火蝾熔样机实现了熔融位置之间的一致加热、均匀的熔体和无污染的加热，以获得准确的分析结果。高速度和高通量高通量的熔样机是高效制备样品的基础。得益于选配的托盘装载器，FORJ火蝾成为市场上拥有出色速度的熔样机，其能够实现生产力提升25%，且所占用的安装面积依然紧凑，保持不变。无忧安装，轻松上手FORJ火蝾熔样机是实验室样品制备的理想省心之选，它易于安装，操作界面友好，方便您快速启动和投入使用。随时随地提供支持马尔文帕纳科的专家十分乐意在整个X射线分析过程中随时随地提供高质量的建议、支持和培训。凭借我们遍布全球的技术和应用支持网络，无论您身在何处，我们都能为您提供服务。

◆国内最先推出的可自动倒样的多头电热熔样机 ◆可4个或6个样同时熔融、自动摇摆、自动倒样 ◆相比高频，无需水冷、也没有电磁场辐射危害 ◆制样速率大于高频，但电耗仅为其一半不到。 ◆The first full automatic multi-sample fusion machine in China even the filling of the fusion sample ◆Up to 4 or 6 samples can be fused simultaneously, shaking and filling automatically ◆No fluid coolant required,no harm of electromagnetic radiation comparing with High Frequency induction ◆More throughput,half energy consumption comparing with High Frequency induction. 简介：玻璃熔融法制成的试样能消除试样的粒度、矿物、偏析等效应，同时也可降低样品元素间的吸收和增强效应，会明显提高分析的精度和准确度，是目前X射线荧光分析的最佳制样方法。对于ICP、AA和湿法化学分析手段，对于难溶样品，熔融方法同样是一种非常完美的制样手段。熔样机随着近几年来国内生产厂家的涌现和推广而在国内得到一定量的应用，但相比先进国家使用率还太低，主要是因为国内的熔样机质量还太差，价格还不够便宜。DY511型全自动多头熔样机是本公司科研人员在公司原有熔样机和当今国际市场上同类制样设备的基础上，研制完成的达到电热熔样机制造技术新高蜂的革命性成果，是在国内最先推出的可自动倒样的全自动多头熔样机。由于其优异的性能和便宜的价格，定将使原来由于经济原因暂不用熔样机的用户也能使用它。DY511型全自动多头熔样机的推出，定将迅速普及熔融制样法，从而提高我国分析界制样的水平，为各行各业带来巨大的经济效益。 Brief Intoduction:The bead fusion method can eliminate the granularity, mineral and segregation effects of the samples, and can reduce the absorption and enhancement effects between the elements in the sample, and hence evidently increase the precision and accuracy of the analysis. This bead fusion method is a optimum sampling method for X ray fluorescence analysis, as well as a perfect sampling method for ICP, AA, and for indissolvable samples in wet chemical analysis.Fusion Machine has a certain amount of domestic applications due to the emergence of domestic manufacturers and promotion in recent years. However, the usage is still too low compared with advanced countries, primarily because of the poor quality of domestic fusion machine and high price.DY511 Automatic Electroheat Fusion Machine is developed by the company’s researchers based on the original fusion machines and the same preparation equipment in current international market, as the revolutionary result reaching to the new peak of electroheat fusion machine manufacturing technology. It is the first fully automatic multi-sample fusion machine with automatic filling of fusion sample. With excellent performances and reasonable price, the fusion machine can be affordable for the users who do not use fusion devices temporarily due to economic reasons. The launch of DY511 Automatic Electroheat Fusion Machine will rapidly popularize bead fusion method, thus improving the sampling quality of domestic analysis industry and bringing tremendous economic benefit for every industry or trade. 特点：◆全自动 – 整个制样过程完全自动进行，包括熔样室的打开、摇篮及模具支架的进出、摇篮的摇摆、将熔样注入成型模具中等。◆高精度 – 采用铂铑热电偶测温，对坩埚和模具中的熔融温度达到准确和精确的测量和控制。◆高均质化 – 坩埚在摇篮中摇摆，保证在最短的时间内有效地搅动熔样，使熔样达到极高的均质化。◆高光洁度 – 熔样成型分开进行，模具的光洁度能长期保持较高（几个月），保证了样品的高光洁度。若坩埚同时兼作模具，则样品在熔融过程中对铂金坩埚的破坏使坩埚内壁会变得粗糙，一般几天得抛光一次（还会损失白金），但由于不能保证抛光和使用的频率，光洁度的一致性就得不到保证。◆高再现性 – 全自动、高精度、高均质化和高光洁度保证了样品的高再现性，从而真正做到经本熔样机同一制样程序制备的不同样品仅是其成分不同而没有其他不同。◆高产量 – 最多可同时熔融4个样品（可根据用户要求增加到6个）。最大制样速率达到36个样品∕小时。◆环保节能 – 无需用水也没有电磁场辐射危害（如高频），无需用气也没有有毒产物（如燃气式），无需大功率电源（如高频）。采用最新的保温材料，最小巧的熔样室设计，使耗能降到最低。◆使用方便 – 菜单式操作，实时温度、过程大屏幕显示，制样过程中无需人工监视。可预先自由设定最多达10个加热制样程序，其加热过程、升温速度、预氧化温度、最终温度、坩埚摇摆幅度和速度、摇摆起始温度、冷却时间、是否用风扇、风量大小等均可预先设定。选定程序后只需按[启动]键即可，真正实现一键操作。◆高可靠性 – 应用单端双螺旋硅碳棒加热，电路、结构简单，保证了熔样机的高可靠性。具有最低启动温度报警，具有过流、过温断电保护并报警，并且过温断电保护采用与加热制样独立的热电偶测温，与加热控制电路一起组成三重保护，使过温断电保护更可靠。◆高性价比 – 价格便宜，维护维修成本极低。摇篮及模具支架采用耐高温合金钢制成, 保证在高温状态下无任何化学反应。精致而紧凑的设计，占用很小的实验室空间。功能强大，性能卓越。是真正的高性价比产品。 Features◆Fully automatic – The whole sample preparation process is carried out automatically, even the filling of the fusion sample in the forming mould.◆Superior accuracy – The temperature is measured by platinum-rhodium thermocouple which can accurately measure and control the fusion temperature in the crucible and forming mould.◆Homogenization – The crucible is shaking in the bracket of the crucible, which ensures the effective agitation in the shortest time and achieves superior homogenization of the fusion sample.◆Smoothness – Fusing and forming are processed separately, so the forming mould smoothness can be maintained for a long term (a few months using 24 hours a day) to ensure the high sample smoothness. If the crucible is also used as the forming mould, the crucible internal wall becomes rough due to the destruction of platinum crucible by sample during fusion process which should be polished after a few days (losing platinum). However, the smoothness homogenization can’t be guaranteed without ensuring the polish and use frequency.◆Superior reproducibility – Fully automatic, superior accuracy, homogenization and smoothness ensure the superior reproducibility of the sample different samples prepared with the same preparation process by this fusion machine are uniformly the same except for the differences in composition.◆Productivity –Up to 4 samples can be fused simultaneously (maximum 6 samples if required by user).The maximum throughput is 36 samples∕hour.◆Environment friendly and energy saving – No water consumption, no electromagnetic field radiation hazardous (such as high frequency), no gas, no toxic products (such as gas type), no high power supply (such as high frequency and previous electroheat). With the newest insulation material and compact fusion chamber design, the energy consumption is the lowest.◆Convenient use –Menu operation real-time temperature and process large-screen display Sample preparation process free of supervision more than 10 preset heating sample preparation programs available Heating process, temperature rise speed, pre-oxidation temperature, final temperature, crucible rotation speed, rotation starting temperature, cooling time, fan or not, air volume can be preset. Press [Start] button after the program selection, one-button operation.◆High reliability – Heating with double helix silicon carbide rod simple circuits and structure ensure the high reliability of the fusion machine With minimum start temperature alarm Automatically switching off power and setting alarm for overcurrent and overheat Independent temperature measurement thermocouples are used for overheat protection and heating control Together with the heating control circuit, they can form treble protection of the system and can make the power switch-off protection for overheat more reliable.◆High performance-to-price ratio – Low price, no consumable. Extremely low maintenance and repair cost. Elegant and compact design occupying small laboratory space, versatility and high performance. Product with real high performance-to-price ratio. 技术指标：1. 加热单元：3根双螺旋单端硅碳棒；2. 最高使用温度：1250℃，连续可调；3. 测温单元：2根铂铑热电偶，最高测温1600℃；4. 容量：同时熔融4个样品（可根据用户要求增加到6个）；5. 制样速率：20～36个样品∕小时；6. 额定功率：5000W；7. 电源：AC380～415V，三相，50～60Hz；8. 尺寸（高′宽′深）：600mm′1100mm′640mm；9. 重量：110kg。 Technical Specifications:1. Heating unit: 3 pieces of double helix ,single-end, silicon carbide rod.2. Maximum usable temperature: 1250℃,continuously adjustable.3. Temperature measurement unit: 2 pieces of platinum-rhodium thermocouple, with maximum measurable temperature 1600℃.4. Capacity: 4 samples simultaneously (maximum 6 samples if required by user).5. Throughput: 24～36 samples/hour.6. Wattage: 5000W.7. Power supply: AC380～415V，三相，50～60Hz.8. Dimension(Height x Width x Depth): 600mm′1100mm′640mm.9. Weight: 110kg. 公司简介：上海宇索实业有限公司（其前身为上海宇索电子科技有限公司）是国内最早成立的专业从事熔融设备研制的企业。公司由长期致力于X荧光分析仪销售服务和研究开发的技术人员合资成立。公司的创办者在长期的X荧光分析仪的销售服务和研究开发中深切地体会到样品制备对荧光分析的重要性，而最好的样品制备方法就是玻璃熔融法，但当时国内所采用的熔融设备均依赖进口，价格又非常昂贵，所以成立了本公司。本公司技术力量雄厚，拥有科技人员多名，其中高级工程师3名，博士1名。公司在2002年成立后的短短一年时间里，就开发完成了填补国内空白的DY501型电热熔融设备。2008年初，本公司最先在国内推出了达到电热熔样机制造技术新高蜂的DY521型全自动熔样机。2013年底，本公司又最先在国内推出了DY511型全自动多头熔样机。至2013年，DY系列电热熔样机的用户已达数百家，并受到用户的一致好评。现正在研究开发金属熔样机等其他熔融设备，并将于近几年陆续推向市场。本公司是样品熔融的专家，分析的好帮手。 Company ProfileShanghai Yusuo Industry Co. Ltd.(formerly Shanghai Yusuo Electronic S&T Co. Ltd.) is the earliest enterprise focusing on manufacturing and researching fusion machine.It is established by the experienced people who focus on the sales, service and research of X-Ray fluorescence analysis instrument many years. Company founder deeply realized the importance of sample preparation on XRF analysis, and the best method of sample preparation is the bead fusion method, but the fusion machine was used in domestic are dependent on imports, the price is very expensive, so the establishment of the company.The company has strong technical strength, with the technological staff, including 3 senior engineers, 1 doctor. The company was founded in 2002 and the span of a year, on the development of the DY501 electroheat fusion machine to fill the domestic blank. At the beginning of 2008, the company was the first in the domestic launch of the electroheat fusion technology to the new peak of DY521 automatic mini electroheat fusion machine. By the end of 2013, the company was the first in the domestic launch of the DY511 automatic electroheat fusion machine which is full automatic multi-sample fusion machine. Till now, DY series of electroheat fusion machine have hundreds of users, and by the user' s consistent high praise. The metal fusion machine and others are under developing, and will be on the market in recent years.Yusuo, the expert on bead fusion, your assistant on analysis. 上海宇索实业有限公司Shanghai Yusuo Industry Co., Ltd. 地址： 上海市凯旋路3500号1号楼2B 邮编： 200030电话： 传真： 网址：http://www.instrument.com.cn/netshow/SH101612/index.aspE-mail:

◆国内最先推出的可自动倒样的多头电热熔样机 ◆可4个或6个样同时熔融、自动摇摆、自动倒样 ◆相比高频，无需水冷、也没有电磁场辐射危害 ◆制样速率大于高频，但电耗仅为其一半不到。 ◆The first full automatic multi-sample fusion machine in China even the filling of the fusion sample ◆Up to 4 or 6 samples can be fused simultaneously, shaking and filling automatically ◆No fluid coolant required,no harm of electromagnetic radiation comparing with High Frequency induction ◆More throughput,half energy consumption comparing with High Frequency induction. 简介：玻璃熔融法制成的试样能消除试样的粒度、矿物、偏析等效应，同时也可降低样品元素间的吸收和增强效应，会明显提高分析的精度和准确度，是目前X射线荧光分析的最佳制样方法。对于ICP、AA和湿法化学分析手段，对于难溶样品，熔融方法同样是一种非常完美的制样手段。熔样机随着近几年来国内生产厂家的涌现和推广而在国内得到一定量的应用，但相比先进国家使用率还太低，主要是因为国内的熔样机质量还太差，价格还不够便宜。DY511型全自动多头熔样机是本公司科研人员在公司原有熔样机和当今国际市场上同类制样设备的基础上，研制完成的达到电热熔样机制造技术新高蜂的革命性成果，是在国内最先推出的可自动倒样的全自动多头熔样机。由于其优异的性能和便宜的价格，定将使原来由于经济原因暂不用熔样机的用户也能使用它。DY511型全自动多头熔样机的推出，定将迅速普及熔融制样法，从而提高我国分析界制样的水平，为各行各业带来巨大的经济效益。 Brief Intoduction:The bead fusion method can eliminate the granularity, mineral and segregation effects of the samples, and can reduce the absorption and enhancement effects between the elements in the sample, and hence evidently increase the precision and accuracy of the analysis. This bead fusion method is a optimum sampling method for X ray fluorescence analysis, as well as a perfect sampling method for ICP, AA, and for indissolvable samples in wet chemical analysis.Fusion Machine has a certain amount of domestic applications due to the emergence of domestic manufacturers and promotion in recent years. However, the usage is still too low compared with advanced countries, primarily because of the poor quality of domestic fusion machine and high price.DY511 Automatic Electroheat Fusion Machine is developed by the company’s researchers based on the original fusion machines and the same preparation equipment in current international market, as the revolutionary result reaching to the new peak of electroheat fusion machine manufacturing technology. It is the first fully automatic multi-sample fusion machine with automatic filling of fusion sample. With excellent performances and reasonable price, the fusion machine can be affordable for the users who do not use fusion devices temporarily due to economic reasons. The launch of DY511 Automatic Electroheat Fusion Machine will rapidly popularize bead fusion method, thus improving the sampling quality of domestic analysis industry and bringing tremendous economic benefit for every industry or trade. 特点：◆全自动 – 整个制样过程完全自动进行，包括熔样室的打开、摇篮及模具支架的进出、摇篮的摇摆、将熔样注入成型模具中等。◆高精度 – 采用铂铑热电偶测温，对坩埚和模具中的熔融温度达到准确和精确的测量和控制。◆高均质化 – 坩埚在摇篮中摇摆，保证在最短的时间内有效地搅动熔样，使熔样达到极高的均质化。◆高光洁度 – 熔样成型分开进行，模具的光洁度能长期保持较高（几个月），保证了样品的高光洁度。若坩埚同时兼作模具，则样品在熔融过程中对铂金坩埚的破坏使坩埚内壁会变得粗糙，一般几天得抛光一次（还会损失白金），但由于不能保证抛光和使用的频率，光洁度的一致性就得不到保证。◆高再现性 – 全自动、高精度、高均质化和高光洁度保证了样品的高再现性，从而真正做到经本熔样机同一制样程序制备的不同样品仅是其成分不同而没有其他不同。◆高产量 – 最多可同时熔融4个样品（可根据用户要求增加到6个）。最大制样速率达到36个样品∕小时。◆环保节能 – 无需用水也没有电磁场辐射危害（如高频），无需用气也没有有毒产物（如燃气式），无需大功率电源（如高频）。采用最新的保温材料，最小巧的熔样室设计，使耗能降到最低。◆使用方便 – 菜单式操作，实时温度、过程大屏幕显示，制样过程中无需人工监视。可预先自由设定最多达10个加热制样程序，其加热过程、升温速度、预氧化温度、最终温度、坩埚摇摆幅度和速度、摇摆起始温度、冷却时间、是否用风扇、风量大小等均可预先设定。选定程序后只需按[启动]键即可，真正实现一键操作。◆高可靠性 – 应用单端双螺旋硅碳棒加热，电路、结构简单，保证了熔样机的高可靠性。具有最低启动温度报警，具有过流、过温断电保护并报警，并且过温断电保护采用与加热制样独立的热电偶测温，与加热控制电路一起组成三重保护，使过温断电保护更可靠。◆高性价比 – 价格便宜，维护维修成本极低。摇篮及模具支架采用耐高温合金钢制成, 保证在高温状态下无任何化学反应。精致而紧凑的设计，占用很小的实验室空间。功能强大，性能卓越。是真正的高性价比产品。 Features◆Fully automatic – The whole sample preparation process is carried out automatically, even the filling of the fusion sample in the forming mould.◆Superior accuracy – The temperature is measured by platinum-rhodium thermocouple which can accurately measure and control the fusion temperature in the crucible and forming mould.◆Homogenization – The crucible is shaking in the bracket of the crucible, which ensures the effective agitation in the shortest time and achieves superior homogenization of the fusion sample.◆Smoothness – Fusing and forming are processed separately, so the forming mould smoothness can be maintained for a long term (a few months using 24 hours a day) to ensure the high sample smoothness. If the crucible is also used as the forming mould, the crucible internal wall becomes rough due to the destruction of platinum crucible by sample during fusion process which should be polished after a few days (losing platinum). However, the smoothness homogenization can’t be guaranteed without ensuring the polish and use frequency.◆Superior reproducibility – Fully automatic, superior accuracy, homogenization and smoothness ensure the superior reproducibility of the sample different samples prepared with the same preparation process by this fusion machine are uniformly the same except for the differences in composition.◆Productivity –Up to 4 samples can be fused simultaneously (maximum 6 samples if required by user).The maximum throughput is 36 samples∕hour.◆Environment friendly and energy saving – No water consumption, no electromagnetic field radiation hazardous (such as high frequency), no gas, no toxic products (such as gas type), no high power supply (such as high frequency and previous electroheat). With the newest insulation material and compact fusion chamber design, the energy consumption is the lowest.◆Convenient use –Menu operation real-time temperature and process large-screen display Sample preparation process free of supervision more than 10 preset heating sample preparation programs available Heating process, temperature rise speed, pre-oxidation temperature, final temperature, crucible rotation speed, rotation starting temperature, cooling time, fan or not, air volume can be preset. Press [Start] button after the program selection, one-button operation.◆High reliability – Heating with double helix silicon carbide rod simple circuits and structure ensure the high reliability of the fusion machine With minimum start temperature alarm Automatically switching off power and setting alarm for overcurrent and overheat Independent temperature measurement thermocouples are used for overheat protection and heating control Together with the heating control circuit, they can form treble protection of the system and can make the power switch-off protection for overheat more reliable.◆High performance-to-price ratio – Low price, no consumable. Extremely low maintenance and repair cost. Elegant and compact design occupying small laboratory space, versatility and high performance. Product with real high performance-to-price ratio. 技术指标：1. 加热单元：3根双螺旋单端硅碳棒；2. 最高使用温度：1250℃，连续可调；3. 测温单元：2根铂铑热电偶，最高测温1600℃；4. 容量：同时熔融4个样品（可根据用户要求增加到6个）；5. 制样速率：20～36个样品∕小时；6. 额定功率：5000W；7. 电源：AC380～415V，三相，50～60Hz；8. 尺寸（高′宽′深）：600mm′1100mm′640mm；9. 重量：110kg。 Technical Specifications:1. Heating unit: 3 pieces of double helix ,single-end, silicon carbide rod.2. Maximum usable temperature: 1250℃,continuously adjustable.3. Temperature measurement unit: 2 pieces of platinum-rhodium thermocouple, with maximum measurable temperature 1600℃.4. Capacity: 4 samples simultaneously (maximum 6 samples if required by user).5. Throughput: 24～36 samples/hour.6. Wattage: 5000W.7. Power supply: AC380～415V，三相，50～60Hz.8. Dimension(Height x Width x Depth): 600mm′1100mm′640mm.9. Weight: 110kg. 公司简介：上海宇索实业有限公司（其前身为上海宇索电子科技有限公司）是国内最早成立的专业从事熔融设备研制的企业。公司由长期致力于X荧光分析仪销售服务和研究开发的技术人员合资成立。公司的创办者在长期的X荧光分析仪的销售服务和研究开发中深切地体会到样品制备对荧光分析的重要性，而最好的样品制备方法就是玻璃熔融法，但当时国内所采用的熔融设备均依赖进口，价格又非常昂贵，所以成立了本公司。本公司技术力量雄厚，拥有科技人员多名，其中高级工程师3名，博士1名。公司在2002年成立后的短短一年时间里，就开发完成了填补国内空白的DY501型电热熔融设备。2008年初，本公司最先在国内推出了达到电热熔样机制造技术新高蜂的DY521型全自动熔样机。2013年底，本公司又最先在国内推出了DY511型全自动多头熔样机。至2013年，DY系列电热熔样机的用户已达数百家，并受到用户的一致好评。现正在研究开发金属熔样机等其他熔融设备，并将于近几年陆续推向市场。本公司是样品熔融的专家，分析的好帮手。 Company ProfileShanghai Yusuo Industry Co. Ltd.(formerly Shanghai Yusuo Electronic S&T Co. Ltd.) is the earliest enterprise focusing on manufacturing and researching fusion machine.It is established by the experienced people who focus on the sales, service and research of X-Ray fluorescence analysis instrument many years. Company founder deeply realized the importance of sample preparation on XRF analysis, and the best method of sample preparation is the bead fusion method, but the fusion machine was used in domestic are dependent on imports, the price is very expensive, so the establishment of the company.The company has strong technical strength, with the technological staff, including 3 senior engineers, 1 doctor. The company was founded in 2002 and the span of a year, on the development of the DY501 electroheat fusion machine to fill the domestic blank. At the beginning of 2008, the company was the first in the domestic launch of the electroheat fusion technology to the new peak of DY521 automatic mini electroheat fusion machine. By the end of 2013, the company was the first in the domestic launch of the DY511 automatic electroheat fusion machine which is full automatic multi-sample fusion machine. Till now, DY series of electroheat fusion machine have hundreds of users, and by the user' s consistent high praise. The metal fusion machine and others are under developing, and will be on the market in recent years.Yusuo, the expert on bead fusion, your assistant on analysis.