竺洪振、杨正红:破解原料药及辅料比表面积测定的脱气难题!
p style="text-indent: 32px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="text-align: justify text-indent: 28px line-height: 114% background: rgb(255, 255, 255) font-family: 宋体 "药物粉体是大部分药物制剂的主体,其疗效不仅取决于药物的种类,而且很大程度上还取决于组成药剂的粉体性能,包括粒度、形状、表面特性等各类参数。药物粉体的比表面积和孔径关系到粉末颗粒的粒径、吸湿性、溶解度、溶出度和压实度等性能,不仅如此,比表面在粉体的流动和粘结性能中,也具有举足轻重的作用,最终影响到药物的生物利用度。/spanspan style="text-align: justify text-indent: 28px font-family: Calibri line-height: 114% letter-spacing: 1px font-size: 14px "span style="font-size: 16px font-family: 宋体 "在此背景下,《中国药典》/span2020span style="font-size: 16px font-family: 宋体 "版四部通则增加和修订了多项理化分析内容,包括比表面积测定法和固体密度测定法等物理参数的测定。/span/span/pp style="text-indent: 30px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="line-height: 114% letter-spacing: 1px font-size: 16px font-family: 宋体 "用气体吸附法进行比表面和孔径分布测定,对于大多数制药行业的用户还比较陌生。/spanspan style="line-height: 114% font-size: 16px font-family: 宋体 "随着近些年纳米科技的发展和新型药品的研发成功,需要进行比表面积和孔径分析的材料越来越多,不再仅仅局限于传统的多孔材料、催化材料、粉体材料,/spanspan style="font-size: 16px font-family: 宋体 "众所周知,/spanspan style="font-family: Calibri font-size: 14px "span style="font-size: 16px font-family: 宋体 "药物的比表面积分析已经进入/span2020span style="font-size: 16px font-family: 宋体 "版中国药典/span/spanspan style="line-height: 114% font-size: 16px font-family: 宋体 "。/span/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: 宋体 line-height: 114% font-size: 14px "span style="font-size: 16px font-family: 宋体 "例如,/spanCOFspan style="font-size: 16px font-family: 宋体 "材料。/span/spanspan style="font-family: Calibri line-height: 114% font-size: 14px "2007span style="font-size: 16px font-family: 宋体 "年/spanspan style="font-size: 16px font-family: Calibri ", Yaghi/spanspan style="font-size: 16px font-family: 宋体 "团队在不断研究金属有机框架聚合物(/spanspan style="font-size: 16px font-family: Calibri "MOF/spanspan style="font-size: 16px font-family: 宋体 ")后,首次报道了共价有机框架聚合物(/spanspan style="font-size: 16px font-family: Calibri "COF/spanspan style="font-size: 16px font-family: 宋体 ")。这种低密度、高比表面、易于修饰改性和功能化的一经问世,短短十余年之间,就在气体储存与分离、非均相催化、储能材料、光电、传感以及药物传递等领域展现出优异的应用前景,并且已经发展成为一种纳米药物载体。/span/span/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: Calibri line-height: 114% font-size: 14px "span style="font-size: 16px font-family: 宋体 "但是,困扰很多检测和科研人员多年的问题是:/span“span style="font-size: 16px font-family: 宋体 "如何判断我们样品的比表面积和孔径分析结果的准确性/spanspan style="font-size: 16px font-family: Calibri "”/spanspan style="font-size: 16px font-family: 宋体 "?想要回答这个问题,我们就不得不先探讨/span/spanspan style="line-height: 114% font-size: 16px font-family: 宋体 ":/spanstrongspan style="font-family: Calibri line-height: 114% font-size: 14px "“span style="font-size: 16px font-family: 宋体 "如何正确的制备样品/spanspan style="font-size: 16px font-family: Calibri "”/spanspan style="font-size: 16px font-family: 宋体 "?/span/span/strongstrongspan style="line-height: 114% font-size: 16px font-family: 宋体 "或者/span/strongstrongspan style="font-family: Calibri line-height: 114% font-size: 14px "“span style="font-size: 16px font-family: 宋体 "怎样制备样品才能确保接下来的分析数据更可靠呢/spanspan style="font-size: 16px font-family: Calibri "”/spanspan style="font-size: 16px font-family: 宋体 "?/span/span/strongstrong/strong/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 14px font-family: 宋体, SimSun "span style="font-size: 16px font-family: 宋体 "在进行气体吸附实验或测定之前,必须清除固体样品表面及孔道中的水汽和杂质气等污染物。这个样品制备过程一般在真空加热的条件下进行,被称作脱气。由于脱气温度、脱气时间以及脱气真空度都与比表面积值有关,所以不同的脱气条件,会导致不同的/span BET span style="font-size: 16px font-family: 宋体 "比表面积结果。/span/span/ph1 label="标题居中" style="font-size: 32px font-weight: bold border-bottom: 2px solid rgb(204, 204, 204) padding: 0px 4px 0px 0px text-align: center margin: 0px 0px 20px "span style="font-family: 宋体, SimSun font-size: 18px color: rgb(0, 176, 240) "strongspan style="font-size: 18px font-family: 宋体 "如何避免因样品处理引起的误差?/span/strong/span/h1p style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: 宋体 font-size: 14px "span style="font-size: 16px font-family: 宋体 "因为/span99%span style="font-size: 16px font-family: 宋体 "的原料药及辅料都是有机化合物,比表面积低,容易受热分解,所以,/span/spanspan style="font-size: 16px font-family: 宋体 "在测定吸附等温线之前进行真空脱气,不仅需要去除样品表面和孔道中的物理吸附物质,同时还需避免样品表面发生不可逆的变化。/span/spanspan style="font-family: 宋体, SimSun " /span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "img style="max-width:100% max-height:100% " src="https://img1.17img.cn/17img/images/202007/uepic/e9a957ec-8de4-424a-b68d-7a99eab71b95.jpg" title="1.jpg" alt="1.jpg"//pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "strongspan style="font-family: 华文仿宋 font-size: 12px "span style="font-size: 16px font-family: 华文仿宋 "图/span1 iBox 26 全自动智能脱气站功能说明/span/strong/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-size: 16px font-family: 宋体 "一种可行的方法是通过热重分析、光谱法或使用不同时间和温度脱气条件的试验找到脱气的最高温度。如今,理化联科/spanspan style="font-family: Calibri font-size: 14px "iBox 26/spanspan style="font-size: 16px font-family: 宋体 "全自动智能脱气站的真空脱气技术提供了另外一条解决途径。该技术/spanspan style="font-family: Calibri font-size: 14px "span style="font-size: 16px font-family: 宋体 "通过内置压力传感器测定残余气体压力,如果压力在/span15span style="font-size: 16px font-family: 宋体 "分钟内保持稳定值,即可自动判断脱气完成/spanspan style="font-size: 16px font-family: Calibri "(/spanspan style="font-size: 16px font-family: 宋体 "图/spanspan style="font-size: 16px font-family: Calibri "2)/spanspan style="font-size: 16px font-family: 宋体 "。该程序还可以确定系统有无泄漏(图/spanspan style="font-size: 16px font-family: Calibri "3/spanspan style="font-size: 16px font-family: 宋体 ")。/span/span/span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "img style="max-width:100% max-height:100% " src="https://img1.17img.cn/17img/images/202007/uepic/29accef5-5d0f-457b-a525-3abba86166ba.jpg" title="2.jpg" alt="2.jpg"//pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"图/span2 iBox 26 的脱气压力、脱气温度、升温速率和保温时间控制/span/strongstrong/strong/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"img style="max-width:100% max-height:100% " src="https://img1.17img.cn/17img/images/202007/uepic/8d4566eb-25d4-48ed-a09c-87884ed484b3.jpg" title="3.png" alt="3.png"//span/strong/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"图/span3 脱气压力变化走向示意图/span/strong/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体 "该脱气站内置了压力传感器,可以自动控温、控压,并且具有高温炉全自动升降功能。可以帮助制药行业用户减少人工干预,保证样品处理条件的一致性。/span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体 "img style="max-width: 100% max-height: 100% width: 300px height: 400px " src="https://img1.17img.cn/17img/images/202007/uepic/1afc08ab-0419-4543-939a-1368f4783772.jpg" title="4.jpg" alt="4.jpg" width="300" height="400" border="0" vspace="0"//span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"图/span4 iBox 26 的内部纵览/span/strongstrong/strong/pp style="text-indent: 24px line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"样品管触底缓冲装置可以避免样品管在电梯上升过程中的撞击,保证样品管接触炉底,均匀受热/span/span/strongstrong/strong/pp style="text-indent: 24px line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"br//span/span/strong/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "script src="https://p.bokecc.com/player?vid=B8658404B449411B9C33DC5901307461&siteid=D9180EE599D5BD46&autoStart=false&width=600&height=350&playerid=621F7722C6B7BD4E&playertype=1" type="text/javascript"/scriptspan style="font-size: 16px font-family: 宋体, SimSun "strongspan style="color: rgb(192, 0, 0) font-size: 16px font-family: 宋体 "(点击观看自动电梯高温炉视频)/span/strong/span/ph1 label="标题居中" style="font-size: 32px border-bottom: 2px solid rgb(204, 204, 204) padding: 0px 4px 0px 0px text-align: center margin: 0px 0px 20px "span style="font-family: 宋体, SimSun font-size: 18px color: rgb(0, 176, 240) "strongspan style="font-size: 18px font-family: 宋体 "初学者如何判断脱气完成?/span/strong/span/h1p style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-size: 16px font-family: 宋体 "即使是从未接触过的样品或初次使用比表面和孔径分析仪的操作人员,也可以采用/spanspan style="font-family: Calibri font-size: 14px "iBox 26/spanspan style="font-family: 宋体 font-size: 14px "span style="font-size: 16px font-family: 宋体 "提供的/spanAIspan style="font-size: 16px font-family: 宋体 "脱气完成自动判断模式来处理样品(图/span6span style="font-size: 16px font-family: 宋体 ")。根据/span/spanspan style="font-family: " times="" new="" font-size:=""ISO9277-2010span style="font-size: 16px font-family: 宋体 ",/span/spanspan style="font-size: 16px font-family: 宋体 "脱气温度会在压力控制下递进,以避免样品受热分解。当软件判断脱气完成后,自动终止脱气,避免人为因素,防止样品结构受损。这对制药行业尤为重要。/span/span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-size: 16px font-family: 宋体 "img style="max-width:100% max-height:100% " src="https://img1.17img.cn/17img/images/202007/uepic/40ba4d51-1f02-4d28-a166-5ef90d7bbd0a.jpg" title="5.jpg" alt="5.jpg"//span/span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "strongspan style="font-family: 华文仿宋 font-size: 12px "span style="font-size: 16px font-family: 华文仿宋 "/span/span/strong/span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"图/span/span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px"5/span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px" iBox 26 的压力控制温度递进,自动判断脱气完成终点/span/strong/ph1 label="标题居中" style="font-size: 32px font-weight: bold border-bottom: 2px solid rgb(204, 204, 204) padding: 0px 4px 0px 0px text-align: center margin: 0px 0px 20px "span style="font-family: 宋体, SimSun color: rgb(0, 176, 240) font-size: 18px "strongspan style="color: rgb(0, 176, 240) font-family: 宋体 "孔道坍塌风险如何解?/span/strong/span/h1p style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: 宋体 font-size: 14px "MOFspan style="font-size: 16px font-family: 宋体 "和/spanspan style="font-size: 16px font-family: " times="" new=""COF/spanspan style="font-size: 16px font-family: 宋体 "等都属于敏感性材料,因为快速加热会因强烈的蒸汽释放而损坏脆弱的结构,因此/span/spanspan style="font-size: 16px font-family: 宋体 "脱气不当容易导致孔道坍塌。/spanstrongspan style="font-family: 华文仿宋 font-size: 12px "iBox/span/strongspan style="font-family: 宋体 font-size: 14px "span style="font-size: 16px font-family: 宋体 "压力控制加热程序可以根据真空条件下脱气过程中多孔材料产生的气体压力来改变加热速率,通过压力与/spanPFCspan style="font-size: 16px font-family: 宋体 "自动抽空速率调节的联动保持压力的稳定。当由于样品表面脱附的物质超过固定的压力极限/spanspan style="font-size: 16px font-family: " times="" new=""P/span/spansubspan style="font-family: 宋体 font-size: 14px vertical-align: sub "L/span/subspan style="font-size: 16px font-family: 宋体 ",升温停止,温度保持恒定,直到压力降至极限以下,此时系统继续升温,该程序可以有效避免微介孔中的结构变化。/span/spanspan style="font-family: 宋体, SimSun " /span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-family: 宋体, SimSun "img style="max-width:100% max-height:100% " src="https://img1.17img.cn/17img/images/202007/uepic/6ec59f46-0fa4-4376-a981-63df6a1a8e1f.jpg" title="6.jpg" alt="6.jpg"//span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-family: 宋体, SimSun "/span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"图/span/span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px"6/span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px" /span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px" /span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px"iBox26是是理化联科iPore 400/600全自动比表面积和孔径分析仪的标准配置(图/span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px"6/span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"),/span/span/strong/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"并可根据样品脱气需求选择机械泵(标配)或分子泵(选配/span)/span/strong/ph1 label="标题居中" style="font-size: 32px font-weight: bold border-bottom: 2px solid rgb(204, 204, 204) padding: 0px 4px 0px 0px text-align: center margin: 0px 0px 20px "span style="font-size: 18px "span style="font-family: 宋体, SimSun color: rgb(0, 176, 240) "strongspan style="line-height: 114% font-family: 宋体 "脱气温度过高/span/strongstrongspan style="line-height: 114% font-family: 宋体 "的/span/strongstrongspan style="line-height: 114% font-family: 宋体 "分解/span/strongstrongspan style="line-height: 114% font-family: 宋体 "风险如何解?/span/strong/span/span/h1p style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-size: 16px font-family: 宋体 "药品多为有机化合物,大部分软化温度和玻璃化温度都较低,通过脱气站进行预处理时必须控制好脱气温度,/spanspan style="font-family: Calibri color: rgb(255, 0, 0) font-size: 14px " /spanspan style="font-family: Calibri font-size: 14px "span style="font-size: 16px font-family: 宋体 "例如,美国药典(/spanUSPspan style="font-size: 16px font-family: 宋体 ")规定硬脂酸镁的脱气温度为/spanspan style="font-size: 16px font-family: Calibri "40 /span/spanspan style="font-family: 宋体 font-size: 14px "℃/spanspan style="font-size: 16px font-family: 宋体 "。但是,很多/spanspan style="font-family: Calibri font-size: 14px "span style="font-size: 16px font-family: 宋体 "脱气站加热包或陶瓷炉的控温允许误差就达到/span10 /spanspan style="font-family: 宋体 font-size: 14px "℃/spanspan style="font-size: 16px font-family: 宋体 ",药品和辅料的脱气温度过高容易导致分解,这也是为医药行业样品表面处理的实际应用难题。/span/spanspan style="font-family: 宋体, SimSun " /span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-family: 宋体, SimSun "img style="max-width:100% max-height:100% " src="https://img1.17img.cn/17img/images/202007/uepic/56fba5cb-d04a-4c0a-a151-aaf4fa5fcb7e.jpg" title="7.jpg" alt="7.jpg"//span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "strongspan style="font-size: 16px font-family: 华文仿宋 "/span/strong/span/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"图/span/span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px"7/span/strongstrongspan style="font-family: 华文仿宋 font-size: 12px" iBox 26 的软件控制界面/span/strongstrong/strong/pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "strongspan style="font-family: 华文仿宋 font-size: 12px"span style="font-family:华文仿宋"从中可以实时监测加热温度、样品温度、真空度和各个脱气站的阀门状态/span/span/strong/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: 宋体 font-size: 14px "iBox 26/spanspan style="font-family: " times="" new="" font-size:=""span style="font-size: 16px font-family: 宋体 "内置/span32/spanspan style="font-size: 16px font-family: 宋体 "位电子电路和全触屏设计,触控电脑预装图形化操控软件,/spanspan style="font-family: 宋体 font-size: 14px "span style="font-size: 16px font-family: 宋体 "控温精度达到/span0.02span style="font-size: 16px font-family: 宋体 "℃/span/spanspan style="font-size: 16px font-family: 宋体 "。另外/spanspan style="font-family: " times="" new="" font-size:=""PFCspan style="font-size: 16px font-family: 宋体 "流控系统精确控制抽空和回填气速率,/span/spanspan style="font-family: 宋体 font-size: 14px "span style="font-size: 16px font-family: 宋体 "可以解决/spanCOFspan style="font-size: 16px font-family: 宋体 "类的低密度样品/span/spanspan style="font-size: 16px font-family: 宋体 "抽真空时易倒吸的痛点问题!/spanspan style="font-family: " times="" new="" font-size:="" /span/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-size: 16px font-family: 宋体 "工欲善其事,必先利其器。/spanspan style="text-decoration: underline font-size: 16px font-family: 宋体 "优质的脱气制备单元,是确保比表面积和孔隙分析数据精度的保证。/span/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="text-decoration: underline font-size: 16px font-family: 宋体 "br//span/span/pp style="text-indent: 28px text-align: right line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-family: 宋体, SimSun "—— 2020年7月20日/span/pp style="text-indent: 28px text-align: right line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-family: 宋体, SimSun "br//span/pp style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "strongspan style="font-size: 16px font-family: 宋体 "附:/span/strongstrongspan style="font-family: Calibri font-size: 19px "iBox 26/span/strongstrongspan style="font-size: 16px font-family: 宋体 "全自动智能脱气站产品介绍:/span/strongstrong/strong/span/pp style="margin-left: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: Wingdings font-weight: bold font-size: 14px "l /spanstrongspan style="font-family: Calibri font-size: 14px "span style="font-size: 16px font-family: 宋体 "高达/span500span style="font-size: 16px font-family: 宋体 "度/spanspan style="font-size: 16px font-family: Calibri "/600/spanspan style="font-size: 16px font-family: 宋体 "度的脱气温度范围/span/span/strongstrong/strong/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: Calibri font-size: 14px "iBox26span style="font-size: 16px font-family: 宋体 "采用铜合金等温体加热系统替代传统的加热包或陶瓷体,有效保障恒温区控温精度及高温脱气的应用需求。/spanspan style="font-size: 16px font-family: Calibri "iBox26T/spanspan style="font-size: 16px font-family: 宋体 "的温度范围为/spanspan style="font-size: 16px font-family: Calibri "600/spanspan style="font-size: 16px font-family: 宋体 "度,可以满足/span/spanspan style="font-size: 16px font-family: 宋体 "已产生化学吸附样品的脱附要求。/spanstrong/strong/span/pp style="margin-left: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: Wingdings font-weight: bold font-size: 14px "l /spanstrongspan style="font-family: Calibri font-size: 14px "span style="font-size: 16px font-family: 宋体 "多种样品预处理模式的选择,全自动/spanAIspan style="font-size: 16px font-family: 宋体 "智能判定/span/span/strongstrong/strong/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "iBox26span style="font-size: 16px font-family: 宋体 "全自动智能脱气系统允许自定义多种样品预处理模式(/span1span style="font-size: 16px font-family: 宋体 ")/spanAIspan style="font-size: 16px font-family: 宋体 "智能判定模式(/span2span style="font-size: 16px font-family: 宋体 ")传统模式,即固定脱气温度和固定脱气时间(/span3span style="font-size: 16px font-family: 宋体 ")易飞溅样品模式(/span4span style="font-size: 16px font-family: 宋体 ")易沸腾样品模式(/span5span style="font-size: 16px font-family: 宋体 ")自定义模式,以保证获取最佳脱气效果。软件可进行脱气条件一键设定,快速建立适合自身样品的多孔材料预处理方案。/span/span/pp style="margin-left: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: Wingdings font-weight: bold font-size: 14px "l /spanstrongspan style="font-size: 16px font-family: 宋体 "杜绝气路污染,提升脱气效果/span/strongstrong/strong/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-size: 16px font-family: 宋体 "内置/spanspan style="font-family: 宋体 font-size: 14px "10.2/spanspan style="font-family: Calibri font-size: 14px "span style="font-size: 16px font-family: 宋体 "寸触屏/spanPAD,span style="font-size: 16px font-family: 宋体 "可对脱气温度,压力及流量进行编程控制设定,/spanspan style="font-size: 16px font-family: Calibri "PFC/spanspan style="font-size: 16px font-family: 宋体 "流控系统精确控制抽真空和惰气回填的速率,避免超轻和易扬析样品倒吸所引起的气路污染,有效提升样品脱气效果。/span/span/span/pp style="margin-left: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: Wingdings font-weight: bold font-size: 14px "l /spanstrongspan style="font-size: 16px font-family: 宋体 "适用于各种尺寸的样品管/span/strongstrong/strong/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: Calibri font-size: 14px "iBox26span style="font-size: 16px font-family: 宋体 "可定制型加热炉体,适用于各种尺寸的比表面分析仪样品管,具有广泛的兼容性。/span/spanstrong/strong/span/pp style="text-indent: 28px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "strongspan style="font-size: 16px font-family: 宋体 "仪器参数/span/strongstrong/strong/span/ptable border="1" cellspacing="0" style="margin-left: 9px margin-right: 9px border: none" align="center"tbodytr class="firstRow"td width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "型号/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 42px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "iBox26/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 42px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "iBox26T/span/p/td/trtrtd width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "脱气端口/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 56px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: " times="" new="" font-size:=""4/spanspan style="font-family: 宋体 font-size: 14px "个或/spanspan style="font-family: " times="" new="" font-size:=""6/spanspan style="font-family: 宋体 font-size: 14px "个/span/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 42px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: " times="" new="" font-size:=""6/spanspan style="font-family: 宋体 font-size: 14px "个/span/span/p/td/trtrtd width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "脱气温度范围/span/p/tdtd width="170" valign="middle" style="border: 1px solid rgb(0, 0, 0) padding: 5px " align="center"p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: 宋体 font-size: 14px "环境温度至/spanspan style="font-family: " times="" new="" font-size:=""500/spanspan style="font-family: 宋体 font-size: 14px "℃/span/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: 宋体 font-size: 14px "环境温度至/spanspan style="font-family: " times="" new="" font-size:=""600/spanspan style="font-family: 宋体 font-size: 14px "℃/span/span/p/td/trtrtd width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "升温速度/span/p/tdtd width="340" valign="top" colspan="2" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 91px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: " times="" new="" font-size:=""0-50/spanspan style="font-family: 宋体 font-size: 14px "℃/spanspan style="font-family: " times="" new="" font-size:=""//spanspan style="font-family: 宋体 font-size: 14px "分钟/span/span/p/td/trtrtd width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "升温精度/span/p/tdtd width="340" valign="top" colspan="2" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 91px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: " times="" new="" font-size:=""0.1/spanspan style="font-family: 宋体 font-size: 14px "℃控温增量/span/span/p/td/trtrtd width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "温度显示精度/span/p/tdtd width="340" valign="top" colspan="2" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 91px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: " times="" new="" font-size:=""0.01/spanspan style="font-family: 宋体 font-size: 14px "℃/span/span/p/td/trtr style="height:30px"td width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "编程控制/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 91px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "是/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 91px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "是/span/p/td/trtrtd width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "压力传感器/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 63px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: " times="" new="" font-size:=""1000/spanspan style="font-family: 宋体 font-size: 14px " torr/span/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-indent: 2px text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "span style="font-family: " times="" new="" font-size:=""1000/spanspan style="font-family: 宋体 font-size: 14px " torr + 10torr span style="font-size: 16px font-family: 宋体 "(可选)/span/span/span/p/td/trtrtd width="121" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun "真空泵/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun " 机械泵/span/p/tdtd width="170" valign="top" style="border: 1px solid rgb(0, 0, 0) padding: 5px "p style="text-align: justify line-height: 1.5em margin-bottom: 5px margin-top: 5px "span style="font-size: 16px font-family: 宋体, SimSun " 机械泵或分子泵/span/p/td/tr/tbody/tablepbr//pp style="line-height: 1.5em margin-bottom: 5px margin-top: 5px "strong作者简介:/strong/pp style="text-align:center"img src="https://img1.17img.cn/17img/images/202007/uepic/0d301117-b136-4fc6-af57-c8f530f233cf.jpg" title="图片1.jpg" width="664" height="380" border="0" vspace="0" alt="图片1.jpg" style="text-align: center white-space: normal width: 664px height: 380px "//pp style="text-align: center line-height: 1.5em margin-bottom: 5px margin-top: 5px "img style="max-width:100% max-height:100% " src="https://img1.17img.cn/17img/images/202007/uepic/d5ddd933-ee9b-473b-be97-de64a5cb0e39.jpg" title="图片2.jpg" alt="图片2.jpg"//pp style="text-align: right line-height: 1.5em margin-bottom: 5px margin-top: 5px "(声明:本文由理化联科供稿,不代表仪器信息网本网观点)/p