高温高压浮区炉

安东帕MCR Evoluton高温高压流变仪将高压测量单元与 MCR 流变仪配套使用，可以在控制温度和压力的条件下进行流变测试。该系统用于模拟工艺条件、测量样品的压力依赖性以及防止样品超过沸点时蒸发。安东帕提供各种不同的高压测量单元，可确保提供最适合于您应用的解决方案。所有测量单元均可将压力和温度等相关数据直接传输至流变仪软件。应用领域 石油工程：压裂液、原油、酸化压裂液、三次采油 聚合物：超临界发泡 食品：淀粉糊化最高400bar的高压测量池- 温度范围：-30°C 至 300°C- 可用气压或自增压的方式控制压力- 有小容积和大容积测量池可选- 低摩擦球轴承，用于精确的流变测量- 可以选择不锈钢、钛合金或耐腐蚀的哈氏合金版本- 可选配流动测量模式最高1000bar 的高压测量池- 温度范围：室温到 300°C- 可根据需求提供低温选项- 可用气压、液压或自增压方式控制压力- 低摩擦、高耐磨的宝石轴承，甚至可以表征爬杆的黏弹性流体- 钛合金或哈氏合金的材质可提高对腐蚀性材料的抵抗力- 可选配流动测量模式主机型号高温高压测量单元可与MCR102e、MCR302e、MCR702e（单EC马达模式）配套使用。

SciDre高温高压光学浮区炉德国SciDre公司推出的高温高压光学浮区法单晶炉能够提供2200–3000℃以上的生长温度，晶体生长腔压力可达300bar，甚至10-5mbar的高真空。适用于生长各种超导材料单晶，介电和磁性材料单晶，氧化物及金属间化合物单晶等。耐高温、耐高压、高真空、高透光率、拆装简便的样品腔由德国弗劳恩霍夫应用光和精密工程研究所优化设计的高反射率镜面，镜体位置可由高精度步进马达控制调节光阑式光强控制器更方便地调节熔区温度，延长灯泡寿命 仿真化触屏控制软件界面友好，操作简单熔区测温选件测温技术可实时监测加热区温度多路立气路控制选件可控制N2、O2、Ar、空气等的流量和压力， 并可对气体进行比例混合与熔区进行反应气体除杂选件可使高压氩气中的氧含量达到10-12ppm退火选件可对离开熔区的单晶棒提供高达1100℃退火温度和高压氧环境SciDre高温高压光学浮区炉特点● 采用垂直式光路设计● 采用高照度短弧氙灯，多种功率规格可选● 熔区温度：3000℃● 熔区压力：10bar/50bar/100bar/150bar/300bar等多种规格可选● 氧气/氩气/氮气/空气/混合气等多种气路可选● 采用光栅控制技术，加热功率从0-100% 连续可调● 样品腔可实现低至10-5mbar真空环境● 丰富的可升选件SciDre高温高压光学浮区炉技术参数熔区温度：高达2000 - 3000℃以上熔区压力：高至10、50、100、150、300 bar可选熔区真空：1*10-2 mbar或 1*10-5 mbar可选熔区气氛：Ar、O2、N2等可选气体流量：0.25 – 1 L/min流量可控氙灯功率：3kW至15kW可选料棒台尺寸：6.8mm或9.8mm可选拉伸速率：0.1-50mm/h调节速率：0.6 mm/s拉伸尺寸：130mm，150mm，195mm可选旋转速率：0-70rpm用电功率：400V三相 63A 50Hz 主机尺寸：330cm*163cm*92cm （不同规格略有差异）发表文章1. (2020)Single crystal growth and luminescent properties of YSH:Eu scintillator by optical floating zone method Chemical Physics Letters, Volume 738, 1369162. (2020)Anisotropic character of the metal-to-metal transition in Pr4Ni3O10 Phys. Rev. B 101, 1041043. (2020)Synthesis of a New Ruthenate Ba26Ru12O57 Crystals 2020, 10(5), 3554. (2020)Synthesis and characterization of bulk Nd1- SrxNiO2 and Nd1- xSrxNiO3 Phys. Rev. Materials 4, 0844095. (2020)Magnetic phase diagram and magnetoelastic coupling of NiTiO3 Phys. Rev. B 101, 1951226. (2019)High pO2 Floating Zone Crystal Growth of the Perovskite Nickelate PrNiO3 Crystals 2019, 9(7), 3247. (2019)Magnetic properties of high-pressure optical floating-zone grown LaNiO3 single crystals Journal of Crystal Growth Volume 524, 15 October 2019, 1251578. (2019)Bulk single-crystal growth of the theoretically predicted magnetic Weyl semimetals RAlGe (R = Pr, Ce) Phys. Rev. Materials 3, 0242049. (2019)Pushing boundaries: High pressure, supercritical optical floating zone materials discovery Journal of Solid State Chemistry 270 (2019): 705-70910. (2018). Antiferromagnetic correlations in the metallic strongly correlated transition metal oxide LaNiO3. Nature Communications 9:4311. (2017). Single-crystal growth and physical properties of 50% electron-doped rhodate Sr 1.5 La 0.5 RhO 4 Physical Review Materials 1(4), 04400512. (2017). Single crystal growth and structural evolution across the 1st order valence transition in (Pr1-yYy) 1- xCaxCoO3-δJournal of Solid State Chemistry 254, 69-7413. (2017). Large orbital polarization in a metallic square-planar nickelate. Nature Physics 13, 864–86914. (2017). High-Pressure Floating-Zone Growth of Perovskite Nickelate LaNiO3 Single Crystals. Crystal Growth & Design 17(5), 2730-2735.15. (2017). High-pressure optical floating-zone growth of Li(Mn,Fe)PO4 single crystals. Journal of Crystal Growth, 462, 50-59.16. (2016). Evidence for a spinon Fermi surface in a triangular-lattice quantum-spin-liquid candidate. Nature 540, 559–562.17. (2016). Stacked charge stripes in quasi-2D trilayer nickelate La4Ni3O8. PNAS 2016 113 (32) 8945-8950.18. (2016). Single Crystal Growth of Pure Co3+ Oxidation State Material LaSrCoO4. Crystals, 6(8), 98.19. (2015). Floating zone growth of Ba-substituted ruthenate Sr2?xBaxRuO4. Journal of Crystal Growth, 427, 94-98.20. (2015). High pressure floating zone growth and structural properties of ferrimagnetic quantum paraelectric BaFe12O19. APL Materials 3, 062512.21. (2015). Impact of local order and stoichiometry on the ultrafast magnetization dynamics of Heusler compounds. Journal of Physics D: Applied Physics, 48(16), 164016.22. (2014). Brownmillerite Ca2Co2O5: Synthesis, Stability, and Re-entrant Single Crystal to Single Crystal Structural Transitions. Chemistry of Materials, 26(24), 7172-7182.23. (2014). Low-temperature properties of single-crystal CrB2. Physical Review B, 90(6), 064414. (Also on archiv.org.)24. (2014). Effect of annealing on spinodally decomposed Co2CrAl grown via floating zone technique. Journal of Crystal Growth, 401, 617-621. (Also on arxiv.org.)25. (2013). de Haas–van Alphen effect and Fermi surface properties of single-crystal CrB2. Physical Review B, 88(15), 155138. (Also on arxiv.org.)26. (2013). Phase Dynamics and Growth of Co2Cr1–xFexAl Heusler Compounds: A Key to Understand Their Anomalous Physical Properties. Crystal Growth & Design, 13(9), 3925-3934.27. (2011). Exploring the details of the martensite–austenite phase transition of the shape memory Heusler compound Mn2NiGa by hard x-ray photoelectron spectroscopy, magnetic and transport measurements. Applied Physics Letters, 98(25), 252501.28. (2011). Challenges in the crystal growth of Li2CuO2 and LiMnPO4. Journal of Crystal Growth, 318(1), 995-999.29. (2011). Self-flux growth of large EuCu 2 Si 2 single crystals. Journal of Crystal Growth, 318(1), 1043-1047.30. (2010). Influence of heat distribution and zone shape in the floating zone growth of selected oxide compounds. Journal of materials science, 45(8), 2223-2227.31. (2009). Highly ordered, half-metallic Co2FeSi single crystals. Applied Physics Letters, 95(16), 161903.32. (2009). Single-crystal growth of LiMnPO4 by the floating-zone method. Journal of Crystal Growth, 311(5), 1273-1277 (Also on uni-heidelberg.de.)33. (2008). Crystal growth of rare earth-transition metal borocarbides and silicides. Journal of Crystal Growth, 310(7), 2268-2276.用户单位中国科学院物理研究所中国科学院固体物理研究所北京师范大学中山大学南昌大学上海大学北京大学北京航空航天大学......

ScIDre高温高压光学浮区炉-HKZ德国SciDre公司推出的高温高压光学浮区法单晶炉能够提供2200–3000℃以上的生长温度，晶体生长腔压力可达300bar，甚至10-5mbar的高真空。适用于生长各种超导材料单晶，介电和磁性材料单晶，氧化物及金属间化合物单晶等。SciDre高温高压光学浮区炉特点● 采用垂直式光路设计● 采用高照度短弧氙灯，多种功率规格可选● 熔区温度：3000℃● 熔区压力：10bar/50bar/100bar/150bar/300bar等多种规格可选● 氧气/氩气/氮气/空气/混合气等多种气路可选● 采用光栅控制技术，加热功率从0-100% 连续可调● 样品腔可实现低至10-5mbar真空环境● 丰富的可升选件耐高温、耐高压、高真空、高透光率、拆装简便的样品腔由德国弗劳恩霍夫应用光和精密工程研究所优化设计的高反射率镜面，镜体位置可由高精度步进马达控制调节光阑式光强控制器更方便地调节熔区温度，延长灯泡寿命仿真化触屏控制软件界面友好，操作简单熔区测温选件测温技术可实时监测加热区温度多路立气路控制选件可控制N2、O2、Ar、空气等的流量和压力， 并可对气体进行比例混合与熔区进行反应气体除杂选件可使高压氩气中的氧含量达到10-12ppm退火选件可对离开熔区的单晶棒提供高达1100℃退火温度和高压氧环境SciDre高温高压光学浮区炉技术参数熔区温度：高达2000 - 3000℃以上熔区压力：10、50、100、150、300 bar可选熔区真空：1*10-2 mbar或 1*10-5 mbar可选熔区气氛：Ar、O2、N2等可选气体流量：0.25 – 1 L/min流量可控氙灯功率：3kW至15kW可选料棒台尺寸：6.8mm或9.8mm可选拉伸速率：0.1-50mm/h调节速率：0.6 mm/s拉伸尺寸：130mm，150mm，195mm可选旋转速率：0-70rpm用电功率：400V三相 63A 50Hz 主机尺寸：330cm*163cm*92cm （不同规格略有差异）部分用户单位中国科学院物理研究所中国科学院固体物理研究所北京师范大学中山大学南昌大学上海大学北京大学北京航空航天大学......发表文章1. (2020)Single crystal growth and luminescent properties of YSH:Eu scintillator by optical floating zone method Chemical Physics Letters, Volume 738, 1369162. (2020)Anisotropic character of the metal-to-metal transition in Pr4Ni3O10 Phys. Rev. B 101, 1041043. (2020)Synthesis of a New Ruthenate Ba26Ru12O57 Crystals 2020, 10(5), 3554. (2020)Synthesis and characterization of bulk Nd1- SrxNiO2 and Nd1- xSrxNiO3 Phys. Rev. Materials 4, 0844095. (2020)Magnetic phase diagram and magnetoelastic coupling of NiTiO3 Phys. Rev. B 101, 1951226. (2019)High pO2 Floating Zone Crystal Growth of the Perovskite Nickelate PrNiO3 Crystals 2019, 9(7), 3247. (2019)Magnetic properties of high-pressure optical floating-zone grown LaNiO3 single crystals Journal of Crystal Growth Volume 524, 15 October 2019, 1251578. (2019)Bulk single-crystal growth of the theoretically predicted magnetic Weyl semimetals RAlGe (R = Pr, Ce) Phys. Rev. Materials 3, 0242049. (2019)Pushing boundaries: High pressure, supercritical optical floating zone materials discovery Journal of Solid State Chemistry 270 (2019): 705-70910. (2018). Antiferromagnetic correlations in the metallic strongly correlated transition metal oxide LaNiO3. Nature Communications 9:4311. (2017). Single-crystal growth and physical properties of 50% electron-doped rhodate Sr 1.5 La 0.5 RhO 4 Physical Review Materials 1(4), 04400512. (2017). Single crystal growth and structural evolution across the 1st order valence transition in (Pr1-yYy) 1- xCaxCoO3-δJournal of Solid State Chemistry 254, 69-7413. (2017). Large orbital polarization in a metallic square-planar nickelate. Nature Physics 13, 864–86914. (2017). High-Pressure Floating-Zone Growth of Perovskite Nickelate LaNiO3 Single Crystals. Crystal Growth & Design 17(5), 2730-2735.15. (2017). High-pressure optical floating-zone growth of Li(Mn,Fe)PO4 single crystals. Journal of Crystal Growth, 462, 50-59.16. (2016). Evidence for a spinon Fermi surface in a triangular-lattice quantum-spin-liquid candidate. Nature 540, 559–562.17. (2016). Stacked charge stripes in quasi-2D trilayer nickelate La4Ni3O8. PNAS 2016 113 (32) 8945-8950.18. (2016). Single Crystal Growth of Pure Co3+ Oxidation State Material LaSrCoO4. Crystals, 6(8), 98.19. (2015). Floating zone growth of Ba-substituted ruthenate Sr2?xBaxRuO4. Journal of Crystal Growth, 427, 94-98.20. (2015). High pressure floating zone growth and structural properties of ferrimagnetic quantum paraelectric BaFe12O19. APL Materials 3, 062512.21. (2015). Impact of local order and stoichiometry on the ultrafast magnetization dynamics of Heusler compounds. Journal of Physics D: Applied Physics, 48(16), 164016.22. (2014). Brownmillerite Ca2Co2O5: Synthesis, Stability, and Re-entrant Single Crystal to Single Crystal Structural Transitions. Chemistry of Materials, 26(24), 7172-7182.23. (2014). Low-temperature properties of single-crystal CrB2. Physical Review B, 90(6), 064414. (Also on archiv.org.)24. (2014). Effect of annealing on spinodally decomposed Co2CrAl grown via floating zone technique. Journal of Crystal Growth, 401, 617-621. (Also on arxiv.org.)25. (2013). de Haas–van Alphen effect and Fermi surface properties of single-crystal CrB2. Physical Review B, 88(15), 155138. (Also on arxiv.org.)26. (2013). Phase Dynamics and Growth of Co2Cr1–xFexAl Heusler Compounds: A Key to Understand Their Anomalous Physical Properties. Crystal Growth & Design, 13(9), 3925-3934.27. (2011). Exploring the details of the martensite–austenite phase transition of the shape memory Heusler compound Mn2NiGa by hard x-ray photoelectron spectroscopy, magnetic and transport measurements. Applied Physics Letters, 98(25), 252501.28. (2011). Challenges in the crystal growth of Li2CuO2 and LiMnPO4. Journal of Crystal Growth, 318(1), 995-999.29. (2011). Self-flux growth of large EuCu 2 Si 2 single crystals. Journal of Crystal Growth, 318(1), 1043-1047.30. (2010). Influence of heat distribution and zone shape in the floating zone growth of selected oxide compounds. Journal of materials science, 45(8), 2223-2227.31. (2009). Highly ordered, half-metallic Co2FeSi single crystals. Applied Physics Letters, 95(16), 161903.32. (2009). Single-crystal growth of LiMnPO4 by the floating-zone method. Journal of Crystal Growth, 311(5), 1273-1277 (Also on uni-heidelberg.de.)33. (2008). Crystal growth of rare earth-transition metal borocarbides and silicides. Journal of Crystal Growth, 310(7), 2268-2276.