¥10万 - 20万
SPEX SamplePrep
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8000M
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美洲
仪器种类： 研磨机
样品适用： 硬性样品
出料粒度： 0.01mm以下
进样粒度： 无要求
批次研磨量： 100ml
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品牌：SPEX SamplePrep
型号：8000M-230
原产地：美国
仪器介绍
SPEX8000系列高能量球磨机集强力冲击、研磨及振动等高能动作于一体，研磨罐在周期性运动过程中，研磨球高速旋转运动与样品相互撞击，达到研细样品的目的。高效率的球磨机能在较短的时间内向被球磨粉末输送较高的机械能量，使被磨的材料在较短是时间内实现机械合金化（机械活化），甚至形成奈米晶或非晶材料，并减少材料的氧化和污染。
机械合金研磨是一种固态粉末制程技术，主要涉及对粉末粒子在高能球磨机中反复进行熔结、断裂、再熔结的过程。早期该技术主要用于航天领域的镍基、铁基之氧化物散布強化（ oxide-dispersion strengthened）合金上，如今已能用于利用混合纯元素或预合金化粉末来制造平衡与非平衡相合金。非平衡相制造主要有过饱和固溶体、介稳材料、准结晶相和纳米及粉末合金的制备。对涉及机械合金化过程和其变量的探讨，可以回顾这些领域以及有序金属间化合物无序化和材料的机械化学合成的最新进展。通过对粉末研磨过程中易产生杂质和污染物这通常令人头疼问题的分析，建议采用某些方法可以减少甚至避免杂质和污染难题。
技术参数
| 设备尺寸 | 19 in. (48 cm) x 14 in. (36 cm) x 18 in. (46 cm) |
重量 | 76 lbs. net (35 kg); 92 lbs. gross (41 kg) |
电源 | AC230 V/50 Hz 单相 |
电流 | 2A |
电机功率转速 | 1/3马力, 1425转/分钟 @ 50 Hz |
研磨容量 | 样品研磨容量在0.1-10g系列和混合60mL样品 |
工作方式 | 三维振动 |
夹具运行 | 前后2 1/3英寸, 左右1英寸 |
夹具运行速率 | 875次/分钟 [230 V/50 Hz] |
控制 | 开始、暂停、停止按钮;可设定时间，工厂设定100分钟萤幕数位显示，可加购P/N 39450延长到10000分钟 |
应用领域
| 应用领域 | 典型解决方案 |
岩石、金属矿石、合金、沙石、水泥、矿渣、陶瓷、催化钢铁体等 |
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主要特点
8000M Mixer/mill单研磨罐高能量球磨机为全自动控制球磨机(8000D型为双研磨罐)。研磨罐配备多种材质和规格：硬质钢(8001)、不锈钢(8007)、玛瑙(8014)、碳化钨(8004) 、氧化锆陶瓷(8005)、氮化硅(8008)、氧化铝陶瓷(8003)、聚合塑料(8002)。被用来研磨岩石、金属矿石、合金、沙石、水泥、矿渣、陶瓷、催化剂载体和其它100多种脆硬样品。
研磨罐规格
研磨罐规格 | ||||||
Vial P/N | Description | Overall Height w/Cap & Gasket (mm) | Height w/o Cap (mm) | OD (mm) | ID (mm) | Volume (ml) |
3111 | Polystyrene Vial | 27 | 25 | 13.6 | 11.7 | 2.5 |
3114 | Stainless Steel Vial | 27 | 25 | 12.7 | 11.0 | 2.5 |
3116 | Polystyrene Vial | 57 | 51 | 13.4 | 10.7 | 5 |
3117 | Hardened Steel Vial | 27 | 25 | 12.7 | 11.0 | 2.5 |
3118 | Agate Vial | 43 | 33 | 15.9 | 9.5 | 1.6 |
3127 | Hardened Steel Vial | 45 | 42 | 14.9 | 12.4 | 5 |
5004 | Tungsten Carbide Vial | 54 | 48 | 19.0 | 12.5 | 5 |
6133 | Polystyrene Vial | 54 | 51 | 20.1 | 18.0 | 12 |
6133 PC | Polycarbonate Vial | 54 | 51 | 20.1 | 18.0 | 12 |
6134 | Polystyrene Vial | 79 | 76 | 27.9 | 24.9 | 35 |
6135 | Polystyrene Vial | 78 | 76 | 27.9 | 24.9 | 35 |
8001 | Hardened Steel Vial | 76 | 64 | 51.1 | 37.8 | 65 |
8002 | Polystyrene Vial | 72 | 64 | 53.3 | 49.9 | 135 |
8003 | Alumina Ceramic Vial | 70 | 52 | 51.1 | 37.8 | 45 |
8004 | Tungsten Carbide Vial | 62 | 50 | 50.7 | 40.6 | 55 |
8005 | Zirconia Ceramic Vial | 68 | 52 | 57.1 | 38.0 | 45 |
8006 | Methacrylate Vial | 64 | 60 | 50.9 | 37.9 | 55 |
8007 | Stainless Steel Vial | 76 | 64 | 50.8 | 37.8 | 65 |
8008 | Silicon Nitride Vial | 62 | 52 | 57.2 | 37.5 | 45 |
8009 | Round-End-Hardened Steel Vial | 76 | 42 | 58.8 | 37.9 | 35 |
8000M单研磨罐高能量球磨机附件
| : 8005 Zirconia Ceramic Vial Set Vial size 2 1/2 in. diameter x 2 11/16 in. Solid zirconia ceramic vial, cap, and two 1/2 in. balls; seven corprene gaskets. Grinding load approx. 2-8 ml; mixing load approx. 20 ml. 8005A Zirconia Ceramic Ball 1/2 in. diameter. 8007 Stainless Steel Vial Set Vial size 2 1/4 in. diameter x 3 in. Vial body and cap liner made of hardened 440C stainless steel. Two 1/2 in. and four 1/4 in. stainless steel balls are included. Set includes screw-on cap with O-ring to permit wet or dry grinding/mixing. Grinding load 3-10 ml; mixing load approx. 25 ml. 8007B Stainless Steel Ball Set for 8007 Vial Four 1/4 in. and two 1/2 in. stainless steel (440C) balls for 8007 vial set. 8008 Silicon Nitride Vial Set Vial size 2 1/2 in. diameter x 2 11/16 in. solid silicon nitride vial, cap, and two 1/2 in. balls; seven corprene gaskets. Grinding load approx. 2-8 ml; mixing load approx. 20 ml. 8008A Silicon Nitride Ball 1/2 in. diameter. 8009 Round-Ended Hardened Steel Vial Set. Vial Size 2 3/8 in. diameter x 3 in. Hardened steel vial body has grinding chamber with rounded ends for more efficient grinding/mixing. Includes screw-on cap and O-ring for wet or dry use; two 1/2 in. and four 1/4 in. steel balls. Grinding load 3-10 ml; mixing load approximately 25 ml. 8014 Agate Vial Set for 8000 Series Mixer/Mills For dry grinding and mixing. Vial size 2-1/4 in. diameter x 2-3/4 in. All-agate vial body, two slip-on caps, two 1/2 in. agate balls, and eight corprene gaskets. Grinding load 3-8 ml; mixing load approximately 20 ml. 8014A Agate Ball for 8014 Vial 1/2 in. diameter for SPEX SamplePrep 8014 agate vial. 8002 Plastic Vial for 8000 Series Mixer/Mills 2 1/8 in. diameter x 2 1/2 in. Polystyrene body with plastic screw-on cap. Capacity 135 ml; mixing load approx. 50 ml. For use with 3112 or 8006A plastic balls. Sold in units of 100. 8006 Methacrylate Vial Set 2 1/4 in. diameter x 2 5/8 in. Vial body of heavy-gauge methacrylate with methacrylate-lined aluminum screw-on cap. Set includes corprene gasket, two 8006A ( 1/2 in.) and four 3112 ( 3/8 in.) plastic balls. Rugged construction allows grinding of soft materials without metallic contamination. 8006A Methacrylate Balls 1/2 in. diameter, fits all SPEX SamplePrep plastic vials 3/4 in. diameter and larger. Sold in units of 100. 8001 Hardened Steel Vial Set Vial size 2-1/4 in. diameter x 3 in. Vial body and cap liner of hardened tool steel. Set includes screw-on cap with O-ring to allow wet or dry grinding/mixing, two 1/2 in. and four 1/4 in. steel balls. Grinding load 3-10 ml; mixing load approx. 25 ml. 8001B Steel Ball Set Two 1/2 in. and four 1/4 in. steel balls, for SPEX SamplePrep 8001 and 8009 vials. 8003 Alumina Ceramic Vial Set For dry grinding/mixing. Vial size 2-1/4 in. diameter x 2-3/4 in. High purity 99.5% alumina ceramic vial body and two slip-on caps with one 1/2 in. ball; set includes eight corprene gaskets. Grinding load 2-8 ml; mixing load approximately 20 ml. 8003A Alumina Ceramic Ball 1/2 in. diameter for 8003 vial. 8015 Clamp for 8003 Clamps permit slurry grinding in 8003 vial; sold in pairs. One pair required for each 8003. 8004 Tungsten Carbide Vial Set For wet or dry grinding/mixing. Vial size 2-1/4 in. diameter x 2-1/2 in. Tungsten carbide-lined body, two screw-on tungsten-carbide-lined caps, two 7/16 in. tungsten carbide balls, eight corprene gaskets. Grinding load 3-10 ml, mixing load approximately 25 ml. 8004A Tungsten Carbide Ball 7/16 in. diameter for SPEX SamplePrep 5004 and 8004 Tungsten Carbide Vials. 8010 Multiple-Sample Adapter Holds seven vials, each 1/2 in. in diameter, for simultaneous running in 8000M Mixer/Mill. Suitable vials include SPEX SamplePrep 3111, 3114, 3116 and 3117. Vials run at one time should be same length. Can be used in 8000D Mixer/Mill with 3116 vials, or with 3111, 3114, and 3117 vials if 8012 adapter is also used. 8011 Multiple-Sample Adapter. Holds four vials, each 3/4 in. in diameter, for simultaneous running in 8000M Mixer/Mill. Suitable vials include SPEX SamplePrep 3118, 3127, 5004 and 6133. Vials run at one time should be same length. Can be used in 8000D Mixer/Mill with 3118, 5004, and 6133 vials. To use 3127 vials in 8000D, 8012 adapter is also necessary. 8012 Vial Clamp Adapter for the 8000D Mixer/Mill Required when running 8010 adapter with 1 in. vials (3111, 3114, 3117) or 8011 adapter with 3127 vials in the 8000D. 3111 Polystyrene Vial 1/2 in. diameter x 1 in. long. Includes slip-on polyethylene cap. Capacity 2.5 ml; mixing load approx. 1 ml; accepts SPEX SamplePrep 3112 or 3119 plastic balls. Sold in units of 100. 3116 Polystyrene Vial 1/2 in. diameter x 2 in. long. Includes slip-on polyethylene cap. Capacity 5 ml; mixing load approx. 2 ml; accepts SPEX SamplePrep 3112 or 3119 plastic balls. Sold in units of 100. 3116PC Polycarbonate Vial 1/2 in. diameter x 2 in. long. Includes slip-on polyethylene cap. Capacity 5 ml; mixing load approx. 2 ml; accepts SPEX SamplePrep 3112 or 3119 plastic balls. Sold in units of 100. 6133 Polystyrene Vial 3/4 in. diameter x 2 in. long. Includes slip-on polyethylene cap. Capacity 12 ml; mixing load approx. 5 ml; accepts SPEX SamplePrep 3112 or 3119 plastic balls. Sold in units of 100. 6133PC Polycarbonate Vial 3/4 in. diameter x 2 in. long. Includes slip-on polyethylene cap. Capacity 12 ml; mixing load approx. 5 ml. Sold in units of 100. Accepts SPEX SamplePrep 3112, 3119, and 8006A plastic balls. 3114 Stainless Steel Vial Set 1/2 in. diameter x 1 in. long. Made of 303 stainless steel; includes slip-on cap and 1/4 in. stainless steel ball; grinding load 0.2-0.6 ml, mixing load 1 ml. 3117 Hardened Tool 1/2 in. diameter x 1 in. long. Made of Worpliss tool steel. Includes slip-on cap and 1/4 in. steel ball. Grinding load 0.2 - 0.6 ml, mixing load 1 ml. Four balls per set. 3127 Hardened Tool Steel Vial Set 3/4 in. diameter x 1 7/8 in. long. Made of Worpliss tool steel; includes center cylinder with two slip-on caps and 1/4 in. steel ball. Grinding load 0.5-1.0 ml, mixing load 2 ml. 3118 Agate Vial Set Handmade from flawless Brazilian agate; must be run inside cushioned SPEX SamplePrep 6133 vial (included). Includes stopper and 1/4 in. agate ball (3118A) Grinding load 0.2 - 0.6 ml, mixing load 1 ml. 5004 Tungsten Carbide-Lined Vial Set 3/4 in. diameter x 2 1/8 in. long. Includes two slip-on Delrin® caps with tungsten carbide inserts, six disposable methacrylate center cylinders, and two 5/16 in. tungsten carbide balls(5004A). Grinding load 0.5-1.5 ml; mixing load 3 ml. |
