逸出气体分析

《逸出气体分析》分册着重阐述TGA-FTIR和TGA-MS两种联用技术。第一部分讲述这两种技术的基本原理，也包括一些实际内容和介绍图谱的解析。第二部分讨论用TGA-FTIR和TGA-MS做的15项不同的应用，以及两个相对较少使用的TMA和MS联用技术的应用。

目录

缩写和简称Abbreviations and Acronym.....................................1

TGA-EGA概述Introduction to TGA-EGA......................................2

TGA-MS..................................... .............................4

TGA-FTIR..................................... ...........................12

应用介绍Introduction to the Applications.................................23

应用一览Application List..................................... ...........24

1乙酰水杨酸分解Decomposition of Acetylsalicylic Acid..................25

2BHET的热裂解Thermal Degradation of BHET..............................28

3加热速率对MS响应的影响Influence of the Heating Rate on MS Response…31

4工业月桂醇的分解Decomposition of Technical Lauryl Alcohol………………34

5药物中残留溶剂的检定Detection of Residual Solvents in a Pharmaceutical Substance..................................... ............................37

6一水草酸钙（演示品）分解Decomposition of Calcium Oxalate Monohydrate(Tutorial) ..................................... ...............39

7样品量对MS灵敏度的影响Influence of Sample Weight on MS Sensitivity…42

8五水硫酸铜（演示品）分解Decomposition of Copper Sulfate Pentahydrate(Tutorial) ..................................... ..............44

9填充有机物沸石的解吸附Desorption of a Zeolite Filled with Organic Matter..47

10PVC粉末的分解Pyrolysis of PVC Powder...................................50

11氟化电缆线的研究Investigation of Fluorinated Cable Wires...............53

12橡胶样品中水杨酸甲酯的检定Detection of Methyl Salicylate in a Sample of Rubber..................................... .................................56

13硅聚合物的裂解Degradation of a Silicone Polymer........................58

14一种胺基树脂的固化和分解Curing and Decomposition of an Amino Resin.....61

15借助热转变和分解鉴别BR和NR橡胶Identification of BR and NR Rubbers by Using Thermal Transitions and Decomposition........................................65

16印刷电路板的分层Delamination of Printed Circuit Boards.................69

17用于包覆发泡剂的聚合物的膨胀和分解Expansion and Decomposition of the Polymer Used to Encapsulate a Blowing Agent..........................................71

参考文献Suggested Literature.................................................73