高效液相色谱-质谱联用测定非布司他片剂中十二烷基硫酸钠含量

文献名： Structural, morphological and optical properties of Bi NPs obtained by laser ablation and their selective detection of L-cysteine 作者： Ramon Gabriel Teixeira Rosaa, Celso de Araujo Duartea , Wido Herwig Schreinera, Ney Pereira Mattoso Filhoa, Arandi Ginane Bezerra Jr.b, Andersson Barisonc, Fernanda Maria Marins Ocamposc a Departamento de Física, Universidade Federal do Paraná Centro Politécnico, CP 19044, 81531-990 Curitiba (PR), Brazil b Departamento Acadêmico de Física, Universidade Tecnológica Federal do Paraná, 80230-901 Curitiba (PR), Brazil c Departamento de Química, Universidade Federal do Paraná Centro Politécnico, CP 19081, 81531-990 Curitiba (PR), Brazil 摘要：In the present work we show the results of the investigation of the properties of bismuth nanoparticles (NPs) obtained by the laser ablation in water. The samples were characterized by various techniques: UV/vis spectroscopy, dynamic light scattering, transmission electron microscopy, X-ray photoelectron spectroscopy, X-ray diffraction, nuclear magnetic resonance and zeta potential. The NPs were metallic and surface oxidated, exhibiting absorption peak at 257 nm due to the surface plasmon resonance. The interaction between the NPs and various amino acids was studied and revealed a selective sensibility to cysteine on a range of concentration from 80 to 720 μM, which we attribute to a dimerization of cysteine to cystine probably complexed to the nanoparticle surface by electrostatic interactions, leading to the modification of the NP absorption spectrum. 关键词：Bismuth; Nanoparticles; Laser ablation; Cysteine

Lipid profiling from complex lipid extracts can be a challenging and time consuming task. The high complexity of samples and co-elution of isobaric or isomeric compounds complicate the confident annotation of lipids. The presented 4D-Lipidomics workflow simplifies and streamlines the annotation and validation process using mobility-enhanced MS data.

智能设备的功能日益多元化，如人脸识别、测距、AR功能等。其中，相机在追求高分辨的 同时，还要求外形小巧、高倍率变焦。 本资料中的数据为测试示例，不代表真实数据，仅供参考。 注意：产品升级后，上述仪器的外观或技术参数可能会有变化。 图2 潜望镜式镜头的示例 通过搭载潜望镜式镜头，可以实现相机的小巧与高倍率变焦。传统相机镜头与智能设备垂直 放置。潜望镜式镜头平行于智能设备安装，从而实现设备的超薄化。此外，变焦倍率越高， 焦距越长，因此，需要一定的纵深空间安放镜头。传统镜头由于是垂直放置，增加焦距则需增加设备厚度，而潜望镜式镜头通过棱镜改变光路方向，将焦距所需要的厚度转化为与智能设备平行的长度，同时实现了超薄化与高倍率变焦。 此次实验，在日立紫外可见近红外分光光度计UH4150上加装微小棱镜测定附件，并使用专用支架※1，测定潜望镜式镜头中的棱镜。

组成电子产品的各种材料，如芯片，屏幕，电路板等电子器件，都需要严格的测试，从而保证电子产品的安全和性能。随着产品的不断进步，消费者的要求不断提升，电子产品的检测需求也随之越来越高，检测项目越来越多。 赛默飞分子光谱产品在电子行业有丰富的应用方案，多年来我们和客户一起应对各种高要求的测试需求，并期待和更多的朋友一起努力，助力我国电子行业持续快速发展。