Formation of CuInS2 Nanoparticles by the Oleylamine Route
简介:Preliminary comparison experiments between microwave
and conventional heating under apparently “similar”
conditions have provided differently sized and shaped
CuInS2 nanoparticles, suggesting the existence of a non
t简介:Preliminary comparison experiments between microwave
and conventional heating under apparently “similar”
conditions have provided differently sized and shaped
CuInS2 nanoparticles, suggesting the existence of a non
thermal microwave effect. However, when repeating those
experiments with Monowave 300 and taking advantage of
the simultaneous temperature monitoring option, it became
evident, that the temperature was not correctly measured
in the initially used monomode microwave reactor, which
led to wrong assumptions. In fact, no evidence for the
existence of a non thermal microwave effect could be
found. However, since Monowave 300 represents a highly
convenient tool for chemical synthesis and additionally
provides accurate temperature measurement,
microwave-assisted reaction processing with internal
temperature monitoring will be the method of choice for
nanomaterial synthesis.详细>