简介:A 1-gram aliquot of solid sample is extracted with ethyl acetate by sonification to
isolate organic halides. A 25 µL aliquot of the extract is either injected or delivered by boat inlet into
a pyrolysis furnace u简介:A 1-gram aliquot of solid sample is extracted with ethyl acetate by sonification to
isolate organic halides. A 25 µL aliquot of the extract is either injected or delivered by boat inlet into
a pyrolysis furnace using a stream of CO /O (or appropriate alternate gas mixture) and the hydrogen 2 2
halide (HX) pyrolysis product is determined by microcoulometric titration.详细>