CTC进样条件 | ||
sample volume:1.0mL | ||
平衡:105℃,45min | ||
250rpm,agitator on 5s,off 2s | ||
syringe temp 115℃ | ||
fill speed:200微升/秒 | ||
pullup del:6.0s | ||
inj。speed。500微升每秒 | ||
pre inj delay:3 s | ||
post inj delay:500ms | ||
syr flushing:6 min | ||
GC runtime:66min | ||
agilent id2mm 直通衬管 |
CTC,气密针顶空进样 | |||||
组分 | 甲醇 | 丙酮 | 异丙醇 | 四氢呋喃 | 甲苯 |
1 | 34.7 | 415.5 | 291.6 | 155.3 | 1425 |
2 | 73.8 | 829.9 | 612 | 288.6 | 1425.5 |
3 | 25.8 | 305.6 | 194.1 | 114.5 | 1007 |
4 | 32.3 | 423.4 | 281.2 | 162.8 | 1501.8 |
5 | 37.8 | 446.9 | 323.7 | 165.8 | 1427.8 |
6 | 28 | 429.5 | 262.8 | 167.3 | 1446.2 |
平均值 | 38.73333333 | 475.1333333 | 327.5666667 | 175.7166667 | 1372.216667 |
RSD% | 45.75863489 | 38.08386291 | 44.52689932 | 33.42014339 | 13.21279566 |