色谱仪型号：戴安ICS-5000，自动进样器AS-DV

软件版本：变色龙6.80

程序设置的目的是：

第1个程序——只分析阴离子，与阴离子分析无关的部件处于关闭状态。

第2个程序——阴阳离子同时分析；

现在的问题是：阴阳离子同时分析是没有问题的。但是第1个程序，在实际操作中出现错误，无法运行。

下面把这两个程序都贴出来，希望有大虾指点一二。

阴离子进样
Column_TC.AcquireExclusiveAccess
Pump_2.Pressure.LowerLimit =  200 [psi]
Pump_2.Pressure.UpperLimit =  3000 [psi]
Pump_2.MaximumFlowRamp =  6.00 [ml/min2]
Pump_2.%A.Equate =  "%A"
Pump_2.%B.Equate =  "%B"
Pump_2.%C.Equate =  "%C"
Pump_2.%D.Equate =  "%D"
Pump_1.Pressure.LowerLimit =  200 [psi]
Pump_1.Pressure.UpperLimit =  3000 [psi]
Pump_1.MaximumFlowRamp =  6.00 [ml/min2]
Pump_1.%A.Equate =  "%A"
Pump_1.%B.Equate =  "%B"
Pump_1.%C.Equate =  "%C"
Pump_1.%D.Equate =  "%D"
EGC_1.CR_TC =  Off
EGC_2.CR_TC =  On
DeliverSpeed =  4.0 [ml/min]
DelayVolume =  125 [μl]
FlushFactor =  10
DeliverSample
Sampler.LoadPosition
DeliverSample Volume=Full
EndSamplePrep
CDet2.Data_Collection_Rate =  5.0 [Hz]
CDet2.Temperature_Compensation =  1.7 [%/°C]
Cell2Heater.Mode = On
Cell2Heater.TemperatureSet =  35.00 [°C]
Column_TC.Mode =  On
Column_TC.TemperatureSet =  30.00 [°C]
Suppressor1.Type =  CSRS_4mm
Suppressor1.CurrentSet =  80 [mA]
Suppressor1.Mode =  off
Suppressor2.Type =  ASRS_4mm
Suppressor2.CurrentSet =  100 [mA]
EGC_1.Concentration =  20.00 [mM]
EGC_1.Mode = Off
EGC_1.Curve =  5
EGC_2.Concentration =  30.00 [mM]
EGC_2.Curve =  5
Pump_1.Flow =  1.200 [ml/min]
Pump_1.Motor = Off
Pump_1.%B =  0.0 [%]
Pump_1.%C =  0.0 [%]
Pump_1.%D =  0.0 [%]
Pump_1.Curve =  5
Pump_2.Flow =  1.200 [ml/min]
Pump_2.%B =  0.0 [%]
Pump_2.%C =  0.0 [%]
Pump_2.%D =  0.0 [%]
Pump_2.Curve =  5

0.000    CDet2.Autozero
                Wait CycleTimeState
                Inject
                CD_2.AcqOn

0.500      BeginOverlap

10.000    CD_2.AcqOff

Column_TC.ReleaseExclusiveAccess
End

阴阳离子同时分析：
Column_TC.AcquireExclusiveAccess
InjectValve_1.LoadPosition
InjectValve_2.LoadPosition
Pump_2.Pressure.LowerLimit =  200 [psi]
Pump_2.Pressure.UpperLimit =  3000 [psi]
Pump_2.MaximumFlowRamp =  6.00 [ml/min2]
Pump_2.%A.Equate =  "%A"
Pump_2.%B.Equate =  "%B"
Pump_2.%C.Equate =  "%C"
Pump_2.%D.Equate =  "%D"
Pump_1.Pressure.LowerLimit =  200 [psi]
Pump_1.Pressure.UpperLimit =  3000 [psi]
Pump_1.MaximumFlowRamp =  6.00 [ml/min2]
Pump_1.%A.Equate =  "%A"
Pump_1.%B.Equate =  "%B"
Pump_1.%C.Equate =  "%C"
Pump_1.%D.Equate =  "%D"
EGC_1.CR_TC =  On
EGC_2.CR_TC =  On
DeliverSpeed =  4.0 [ml/min]
DelayVolume =  125 [μl]
FlushFactor =  10
DeliverSample
Sampler.LoadPosition
DeliverSample Volume=Full
EndSamplePrep
CDet2.Data_Collection_Rate =  5.0 [Hz]
CDet2.Temperature_Compensation =  1.7 [%/°C]
Cell2Heater.Mode = On
Cell2Heater.TemperatureSet =  35.00 [°C]
CDet1.Data_Collection_Rate =  5.0 [Hz]
CDet1.Temperature_Compensation =  1.7 [%/°C]
CellHeater.Mode = On
CellHeater.TemperatureSet =  35.00 [°C]
Column_TC.Mode =  On
Column_TC.TemperatureSet =  30.00 [°C]
Suppressor1.Type =  CSRS_4mm
Suppressor1.CurrentSet =  80 [mA]
  Suppressor2.Type =  ASRS_4mm
Suppressor2.CurrentSet =  100 [mA]
EGC_1.Concentration =  20.00 [mM]
EGC_1.Curve =  5
EGC_2.Concentration =  30.00 [mM]
EGC_2.Curve =  5
Pump_1.Flow =  1.200 [ml/min]
Pump_1.%B =  0.0 [%]
Pump_1.%C =  0.0 [%]
Pump_1.%D =  0.0 [%]
Pump_1.Curve =  5
Pump_2.Flow =  1.200 [ml/min]
Pump_2.%B =  0.0 [%]
Pump_2.%C =  0.0 [%]
Pump_2.%D =  0.0 [%]
Pump_2.Curve =  5

0.000      CDet2.Autozero
                  CDet1.Autozero
                  Wait CycleTimeState
                  Inject
                  CD_2.AcqOn
                  CD_1.AcqOn

0.500      BeginOverlap

12.000    CD_2.AcqOff
                  CD_1.AcqOff
                  Column_TC.ReleaseExclusiveAccess

End