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共有 12 人回复了该问答GC-MS前处理技术-固相动态萃取(SPDE)有用过的吗
 回复pei123发表于:2020/8/9 9:47:28悬赏金额:6积分 状态:未解决
做GC-MS挥发性物质分析,前处理有没有用固相动态萃取(SPDE)的啊? 谁有SPDE的相关资料啊?急急急。。。。。。十分感谢
 回复  1# mcds  回复于:2020-08-09 11:03:28
网上搜的:

SPDE uses an injection needle, the inner surface of which is coated with a polymeric material (e.g. dimethyl polysiloxan). With the help of the syringe, the liquid sample is repeatedly sucked through the needle and pushed out again, with the organic analytes enriching in the polymer film.

Finally, the needle is guided into the hot injector of a gas chromatograph and the thermally desorbing substances transferred to the gc column with the help of a scavenging gas.
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