XRD分析表明是锐钛矿,卡号21-1272
FFT中为什么既有环又有斑点??
环我标出一些,由内至外包括(101)(004)(105)(215)
但是斑点我不明白是什么,没有符合夹角的晶面。就指导~~谢谢~~
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
3.520 100.0 100.0 1 0 1 25.281 12.640 0.1420 1.7850
2.431 10.0 14.0 1 0 3 36.946 18.473 0.2057 2.5846
2.378 20.0 30.0 0 0 4 37.800 18.900 0.2103 2.6422
2.332 10.0 15.0 1 1 2 38.575 19.288 0.2144 2.6943
1.892 35.0 65.0 2 0 0 48.049 24.024 0.2643 3.3209
1.699 20.0 41.0 1 0 5 53.890 26.945 0.2941 3.6962
1.666 20.0 42.0 2 1 1 55.060 27.530 0.3000 3.7703
1.493 4.0 9.0 2 1 3 62.119 31.059 0.3349 4.2084
1.480 14.0 33.0 2 0 4 62.688 31.344 0.3377 4.2431
1.364 6.0 15.0 1 1 6 68.760 34.380 0.3665 4.6061
1.337 6.0 16.0 2 2 0 70.309 35.154 0.3737 4.6967
1.279 2.0 6.0 1 0 7 74.029 37.014 0.3908 4.9107
1.264 10.0 28.0 2 1 5 75.029 37.515 0.3953 4.9673
1.250 4.0 11.0 3 0 1 76.017 38.009 0.3997 5.0229
1.189 2.0 6.0 0 0 8 80.725 40.362 0.4204 5.2827
1.172 2.0 6.0 3 0 3 82.136 41.068 0.4264 5.3588
1.166 6.0 18.0 2 2 4 82.659 41.330 0.4287 5.3868
1.160 4.0 12.0 3 1 2 83.146 41.573 0.4307 5.4128
1.060 2.0 7.0 2 1 7 93.217 46.609 0.4717 5.9275
1.051 4.0 13.0 3 0 5 94.178 47.089 0.4754 5.9743
1.043 4.0 13.0 3 2 1 95.139 47.570 0.4791 6.0207
1.018 2.0 7.0 1 0 9 98.315 49.158 0.4911 6.1709
1.007 2.0 7.0 2 0 8 99.801 49.900 0.4965 6.2395
0.996 2.0 7.0 3 2 3 101.217 50.609 0.5017 6.3040
0.955 4.0 15.0 3 1 6 107.444 53.722 0.5233 6.5758
0.946 4.0 15.0 4 0 0 108.959 54.479 0.5283 6.6390
0.924 2.0 8.0 3 0 7 112.836 56.418 0.5408 6.7956
0.919 2.0 8.0 3 2 5 113.857 56.928 0.5440 6.8355
0.913 2.0 8.0 4 1 1 114.904 57.452 0.5472 6.8759
0.896 4.0 16.0 2 1 9 118.434 59.217 0.5577 7.0078
0.889 2.0 8.0 2 2 8 120.099 60.049 0.5624 7.0677
0.881 2.0 8.0 4 1 3 121.720 60.860 0.5670 7.1246
0.879 2.0 8.0 4 0 4 122.331 61.165 0.5686 7.1457
0.846 2.0 8.0 4 2 0 131.029 65.514 0.5907 7.4234
0.830 2.0 8.0 3 2 7 135.991 67.996 0.6018 7.5628
0.826 4.0 17.0 4 1 5 137.384 68.692 0.6047 7.5994
0.810 2.0 9.0 3 0 9 143.878 71.939 0.6171 7.7551
0.797 4.0 18.0 4 2 4 150.028 75.014 0.6270 7.8796
0.792 2.0 9.0 0 0 12 152.622 76.311 0.6307 7.9253